TA Instruments

AR1756-0016f

15/03/2013 15:20:14

Sample name	ASW Blank coupon#20 + DI + beads 275rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	16 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 15:20:14

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 275.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99600	274.8	-3452.8	10000	20.0	0.4425	0.996	-1125	343.5	-3.276	1803	197.8310	0.01528	247.29	24729	3.411E-3	0.0	0.0
2.0120	275.0	584.13	10000	20.0	0.4070	2.012	190.4	343.7	0.5540	1658	538.3490	0.01404	672.94	67294	3.411E-3	0.0	0.0
3.0120	275.0	577.95	10000	20.0	0.4015	3.012	188.4	343.7	0.5481	1636	763.2990	0.01385	954.12	95412	3.411E-3	0.1	0.1
4.0120	275.0	581.21	10000	20.0	0.4019	4.012	189.4	343.7	0.5511	1638	989.3750	0.01386	1236.7	1.2367E5	3.411E-3	0.1	0.1
5.0120	275.0	564.72	10000	20.0	0.4029	5.012	184.1	343.8	0.5354	1642	1328.6300	0.01389	1660.8	1.6608E5	3.411E-3	0.1	0.1
6.0120	275.0	555.53	10000	20.0	0.4056	6.012	181.1	343.7	0.5268	1652	1554.7900	0.01399	1943.5	1.9435E5	3.411E-3	0.1	0.1
6.9960	275.0	569.39	10000	20.0	0.3995	6.996	185.6	343.7	0.5399	1628	1894.2100	0.01378	2367.8	2.3678E5	3.411E-3	0.1	0.1
7.9960	275.0	562.77	10000	20.0	0.4013	7.996	183.4	343.7	0.5336	1635	2120.3501	0.01384	2650.4	2.6504E5	3.411E-3	0.1	0.1
9.0120	275.0	554.48	10000	20.0	0.4023	9.012	180.7	343.7	0.5258	1639	2459.8899	0.01387	3074.9	3.0749E5	3.411E-3	0.2	0.2
9.9960	275.0	575.12	10000	20.0	0.3981	9.996	187.5	343.7	0.5454	1622	2685.8501	0.01373	3357.3	3.3573E5	3.411E-3	0.2	0.2
10.996	275.0	556.08	10000	20.0	0.3979	10.996	181.3	343.7	0.5273	1621	2912.0801	0.01372	3640.1	3.6401E5	3.411E-3	0.2	0.2
11.996	275.0	556.88	10000	20.0	0.4001	11.996	181.5	343.8	0.5280	1630	3251.3601	0.01380	4064.2	4.0642E5	3.411E-3	0.2	0.2
12.996	275.0	546.50	10000	20.0	0.3971	12.996	178.1	343.8	0.5181	1618	3480.1599	0.01369	4350.2	4.3502E5	3.411E-3	0.2	0.2
13.996	275.0	540.30	10000	20.0	0.4058	13.996	176.1	343.8	0.5122	1653	3816.8501	0.01399	4771.1	4.7711E5	3.411E-3	0.2	0.2
14.996	275.0	554.19	10000	20.0	0.4048	14.996	180.6	343.7	0.5255	1649	4045.3101	0.01396	5056.6	5.0566E5	3.411E-3	0.2	0.2
15.996	275.0	549.59	10000	20.0	0.4062	15.996	179.1	343.8	0.5211	1655	4382.2700	0.01400	5477.8	5.4778E5	3.411E-3	0.3	0.3
17.012	275.0	559.92	10000	20.0	0.4027	17.012	182.5	343.8	0.5309	1641	4608.5200	0.01389	5760.7	5.7607E5	3.411E-3	0.3	0.3
18.012	275.0	560.54	10000	20.0	0.4068	18.012	182.7	343.7	0.5315	1657	4949.9199	0.01403	6187.4	6.1874E5	3.411E-3	0.3	0.3
19.012	275.0	547.71	10000	20.0	0.4058	19.012	178.5	343.8	0.5193	1653	5173.9399	0.01399	6467.4	6.4674E5	3.411E-3	0.3	0.3
19.996	275.0	561.52	10000	20.0	0.4023	19.996	183.0	343.8	0.5324	1639	5401.0298	0.01387	6751.3	6.7513E5	3.411E-3	0.3	0.3
21.012	275.0	577.65	10000	20.0	0.3938	21.012	188.3	343.7	0.5478	1605	5739.3599	0.01358	7174.2	7.1742E5	3.411E-3	0.4	0.4
22.012	275.0	553.80	10000	20.0	0.3964	22.012	180.5	343.8	0.5251	1615	5965.6499	0.01367	7457.1	7.4571E5	3.411E-3	0.4	0.4
22.996	275.0	547.87	10000	20.0	0.4038	22.996	178.6	343.8	0.5195	1645	6306.1099	0.01392	7882.6	7.8826E5	3.411E-3	0.4	0.4
23.996	275.0	566.52	10000	20.0	0.4023	23.996	184.7	343.7	0.5372	1639	6533.2798	0.01388	8166.6	8.1666E5	3.411E-3	0.4	0.4
25.012	275.0	565.82	10000	20.0	0.4042	25.012	184.4	343.8	0.5365	1647	6882.8999	0.01394	8603.6	8.6036E5	3.411E-3	0.4	0.4
25.996	275.0	558.27	10000	20.0	0.4060	25.996	182.0	343.8	0.5293	1654	7096.7500	0.01400	8870.9	8.8709E5	3.411E-3	0.4	0.4
26.996	275.0	550.71	10000	20.0	0.4009	26.996	179.5	343.7	0.5222	1633	7322.9199	0.01382	9153.7	9.1537E5	3.411E-3	0.4	0.4
27.996	275.0	561.99	10000	20.0	0.3924	27.996	183.2	343.7	0.5330	1599	7662.0698	0.01353	9577.6	9.5776E5	3.411E-3	0.5	0.5
28.996	275.0	552.59	10000	20.0	0.4001	28.996	180.1	343.7	0.5240	1630	7889.3999	0.01380	9861.8	9.8618E5	3.411E-3	0.5	0.5
30.000	275.0	553.95	10000	20.0	0.3977	30.000	180.6	343.8	0.5252	1620	8229.0000	0.01371	10286	1.0286E6	3.411E-3	0.5	0.5
31.012	275.0	554.30	10000	20.0	0.3950	31.012	180.7	343.8	0.5256	1609	8453.7695	0.01362	10567	1.0567E6	3.411E-3	0.5	0.5
32.012	275.0	571.68	10000	20.0	0.3960	32.012	186.3	343.8	0.5421	1614	8793.0400	0.01366	10991	1.0991E6	3.411E-3	0.5	0.5
32.996	275.0	551.34	10000	20.0	0.3973	32.996	179.7	343.8	0.5228	1619	9019.4102	0.01370	11274	1.1274E6	3.411E-3	0.5	0.5
34.012	275.0	560.23	10000	20.0	0.4023	34.012	182.6	343.7	0.5313	1639	9245.5801	0.01387	11557	1.1557E6	3.411E-3	0.6	0.6
35.012	275.0	558.38	10000	20.0	0.4040	35.012	182.0	343.7	0.5295	1646	9584.7500	0.01393	11981	1.1981E6	3.411E-3	0.6	0.6
36.012	275.0	563.72	10000	20.0	0.3973	36.012	183.7	343.7	0.5345	1619	9811.0498	0.01370	12264	1.2264E6	3.411E-3	0.6	0.6
37.012	275.0	557.22	10000	20.0	0.3971	37.012	181.6	343.8	0.5283	1618	10150.400	0.01369	12688	1.2688E6	3.411E-3	0.6	0.6
37.996	275.0	543.73	10000	20.0	0.4019	37.996	177.2	343.8	0.5155	1638	10376.400	0.01386	12971	1.2971E6	3.411E-3	0.6	0.6
38.996	275.0	557.88	10000	20.0	0.3960	38.996	181.8	343.8	0.5290	1614	10720.000	0.01366	13400	1.3400E6	3.411E-3	0.6	0.6
39.996	275.0	556.34	10000	20.0	0.3981	39.996	181.3	343.8	0.5275	1622	10944.200	0.01373	13680	1.3680E6	3.411E-3	0.7	0.7
40.996	275.0	568.39	10000	20.0	0.4003	40.996	185.3	343.7	0.5390	1631	11168.200	0.01381	13960	1.3960E6	3.411E-3	0.7	0.7
41.996	275.0	563.21	10000	20.0	0.3958	41.996	183.6	343.7	0.5341	1613	11511.900	0.01365	14390	1.4390E6	3.411E-3	0.7	0.7
42.996	275.0	560.31	10000	20.0	0.3999	42.996	182.6	343.8	0.5313	1629	11733.800	0.01379	14667	1.4667E6	3.411E-3	0.7	0.7
43.996	275.0	570.76	10000	20.0	0.3977	43.996	186.0	343.7	0.5412	1620	12073.200	0.01371	15092	1.5092E6	3.411E-3	0.7	0.7
45.012	275.0	555.55	10000	20.0	0.4013	45.012	181.1	343.8	0.5267	1635	12299.200	0.01384	15374	1.5374E6	3.411E-3	0.8	0.8
45.996	275.0	556.59	10000	20.0	0.3981	45.996	181.4	343.8	0.5278	1622	12638.500	0.01373	15798	1.5798E6	3.411E-3	0.8	0.8
47.008	275.0	566.62	10000	20.0	0.3989	47.008	184.7	343.7	0.5373	1625	12864.600	0.01375	16081	1.6081E6	3.411E-3	0.8	0.8
47.996	275.0	573.43	10000	20.0	0.3967	47.996	186.9	343.7	0.5438	1616	13091.000	0.01368	16364	1.6364E6	3.411E-3	0.8	0.8
48.996	275.0	564.33	10000	20.0	0.3987	48.996	183.9	343.7	0.5352	1624	13430.200	0.01375	16788	1.6788E6	3.411E-3	0.8	0.8
49.996	275.0	560.24	10000	20.0	0.3979	49.996	182.6	343.8	0.5312	1621	13656.300	0.01372	17070	1.7070E6	3.411E-3	0.8	0.8
50.996	275.0	555.63	10000	20.0	0.4033	50.996	181.1	343.7	0.5269	1643	13996.800	0.01391	17496	1.7496E6	3.411E-3	0.8	0.8
51.996	275.0	538.56	10000	20.0	0.4084	51.996	175.5	343.8	0.5106	1664	14221.900	0.01408	17777	1.7777E6	3.411E-3	0.9	0.9
52.996	275.0	559.96	10000	20.0	0.4023	52.996	182.5	343.7	0.5310	1639	14562.300	0.01387	18203	1.8203E6	3.411E-3	0.9	0.9
54.012	275.0	553.73	10000	20.0	0.4015	54.012	180.5	343.7	0.5251	1636	14788.000	0.01385	18485	1.8485E6	3.411E-3	0.9	0.9
55.012	275.0	547.24	10000	20.0	0.4017	55.012	178.4	343.8	0.5189	1637	15013.500	0.01385	18767	1.8767E6	3.411E-3	0.9	0.9
56.016	275.0	554.70	10000	20.0	0.3960	56.016	180.8	343.7	0.5260	1614	15352.700	0.01366	19191	1.9191E6	3.411E-3	0.9	0.9
57.012	275.0	550.11	10000	20.0	0.4058	57.012	179.3	343.8	0.5216	1653	15578.900	0.01399	19474	1.9474E6	3.411E-3	1.0	1.0
57.996	275.0	554.27	10000	20.0	0.4021	57.996	180.7	343.8	0.5255	1638	15918.400	0.01386	19898	1.9898E6	3.411E-3	1.0	1.0
58.996	275.0	557.31	10000	20.0	0.3936	58.996	181.7	343.8	0.5284	1604	16144.400	0.01357	20181	2.0181E6	3.411E-3	1.0	1.0
60.012	275.0	546.17	10000	20.0	0.3971	60.012	178.0	343.8	0.5179	1618	16483.801	0.01369	20605	2.0605E6	3.411E-3	1.0	1.0

